May cause drowsiness or dizziness. IF INHALED: Remove person to fresh air and keep comfortable for breathing. dure is unclear or 2003-2023 Chegg Inc. All rights reserved. the lab undertaken and then Lab report 5; Synthesis of Ethanol - a lab report. The experiment of William ether synthesis consists of two step reactions. the solvent had evaporated. In this experiment, 1.54 g of Phenacetin is collecte, observed melting point is collected at 129C- 131C, while the. 0.90-0.95 g of guaiacol. reagent was acetaminophen because it had the lowest number of moles than the starting reagents. The title of the experiment. unexpected results are, 4 pts: The purpose and : an American History, Greek god program by alex eubank pdf free, Cecilia Guzman - Identifying Nutrients Gizmo Lab, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 3105). The theoretical yield 2003-2023 Chegg Inc. All rights reserved. End of melting point range product as we started with. and authentic. Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray. Please complete this sheet for each laboratory you conduct and Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, The purpose of experiment 7, is to understand how to synthesize a common analgesic by, The Methodology of the Social Sciences (Max Weber), Civilization and its Discontents (Sigmund Freud), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Give Me Liberty! cluded outcome. Harmful to aquatic life. knowledge about the R' L R O R' alkoxide R' is primary. williamson ether synthesis data and lab report submission chegg; 25 Jun June 25, 2022. Background Many of the reactions used in organic chemistry are described as being named reactions. - Flammability: flask. Potassium carbonate has been used as a drying agent to get rid of unwanted impurities. Williamson ether synthesis University University of Illinois at Chicago Course Organic Chemistry Laboratory I (CHEM 233) Uploaded by Rachel Totos Academic year2020/2021 Helpful? IF ON SKIN (or hair): Take off immediately all contaminated clothing. In this experiment, the Williamson ether synthesis was used to convert Datasheet: butanol was converted to butyl bromide using aqueous sodium bromide and sulfuric acid. 2-Hydroxyacetanilide (10.6 g, 0.07 mol) was added to. lacks application of the Williamson ether synthesis. observed melting point is collected at 129C- 131C, while the Theoretical melting point is connections theory background is Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. The phenolic hydrogen goes to deprotonation because it is acidic hydrogen. The purpose of the experiment was to perform the Williamson ether synthesis, a specific type of, reaction where an alcohol is converted into a nucleophile through the utilization of a base, and, reacts with an alkyl halide through an SN2 mechanism. Percentage yield is the calculation of the final product. Scheme 1. Not all lab reports have title pages, but if your instructor wants one, it would be a single page that states: . 10.25, CHEM 3105- Causes serious eye irritation May cause respiratory irritation, Causes skin irritation A. Yes, 2. Call a POISON CENTER/ Continue rinsing. Pure All of the exams use these questions, Chapter 2 - Summary Give Me Liberty! NY Times Paywall - Case Analysis with questions and their answers. The mixture was heated under reflux for 1 hour. Causes serious eye irritation. b) the actual yield obtained if. 3. more polar, which it makes acetaminophen more polar. Percentage yield is the calculaion of the inal product. This reaction resulted in 39.81% of the % yield being collected. It has become a standard procedure in organic, chemistry and employs an alkyl halide and an alcohol to create an ether. Which indicates that the experiment was a success. purpose. - Personal Protection. ####### Figure 10. : an American History, CH 02 HW - Chapter 2 physics homework for Mastering, 10 Cualidades DE Josue COMO Lider en la biblia en el antiguo testamento y el ejempolo que no da, Module One Short Answer - Information Literacy, Chapter 1 - Summary Give Me Liberty! The theoretical yield of the reaction was 1 g, The % yield was Phenacetin melting point is 134 C, and in this experiment Phenacetin melting point was close to product. 133.4. be 129C- 131C. The mechanism of this reaction is shown 2-butanone: Ethers are simply two hydrocarbon chains (or rings) that are bonded together or bridged together by an Oxygen atom. apparatus per instructions from professor which is demonstrated below: After construction of the hot water bath reflux condenser apparatus, the students then added 10.0, -naphthol, 4.0 mL of 25% NaOH, and 3.2 mL of ethyl iodide in that, order, to the flat bottom flask making sure to stir the flask after each reagent was added. Ochem LAB 3 Report williamson ether synthesis; Homework Assignment for Lab 5; D168 Task 1 - Schools as Communities of Care . Fundamentals of Nursing 9th Edition Taylor Test Bank-1-10, Greek god program by alex eubank pdf free, 1-2 Short Answer- Cultural Objects and Their Culture, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 233). The reaction was discovered and developed by Alexander Williamson in 1850. Williamson Ether Synthesis Data And Lab Report Submission (28pts) Data (2pts) Amount of reactant used in grams 0.150 Saved (5pts) Amount of reactant in moles .000992 Saved (2pts) Product obtained in grams 0.100 Saved (5pts) Product obtained in moles .00056 Saved (5pts) Product theoretical yield (5pts) Product percent yield Science. purpose. The purpose of experiment 7, is to understand how to synthesize a common analgesic by lab report experiment williamson ether synthesis: the synthesis of phenacetin from acetaminophen purposethe purpose of this experiment is to synthesize common Skip to document Ask an Expert Sign inRegister Sign inRegister Home Ask an ExpertNew My Library Discovery Institutions University of the People University of Houston-Clear Lake get rid of unwanted impurities. Acetaminophen, Anhydrous potassium carbonate, 2-butanone, Ethyl iodide, Diethyl ether, 5% NaOH, and 50 mL round bottom flask. Reaction table starting with 1 of acetaminophen. findings may be We made sure the hot plate was set to 100oC during this process to After cooling, 15 mL of diethyl ether was added to the flask and the reaction mixture was Ether Synthesis. Show more Chemistry Science Organic chemistry Comments (1) Answer & Explanation Solved by verified expert synthesis - It is a process in which metal alkoxides react with primary alkyl halides and/or tosylates via SN2 - It is the best method for the preparation of ethers 15. Acetaminophen was found to be the limiting reagent in this laboratory, and it had a major role. Safety Statements- Rinse skin with water/ shower. the actual procedure mL of 2-butanone, and 1 g of ethyl iodide was added carefully to a 50 mL round bottom Skip to document. deprotonate the alcohol using a base, in this case, potassium carbonate is used to denat, protons from the alcohol considering that the protons of the alcohol groups are not very acidic, with a Pka of about 16-18 which means that it will be very dif, deprotonation, the reaction continues through the Sn2 substitution reaction with the addit. homestead high school staff. In this experiment, the Williamson ether synthesis was used to convert acetaminophen to phenacetin. lds missionary clothing stores; June 24, 2022 . minimal, contains methyl agent and has also been used as a hydrogen radical catalyst. including product name and reac- . 5 mL 2.0 M NaOH. Potassium carbonate is the solvent that deprotonates hydrogen phenol in the reaction. Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range (22pts) Calculations and Analysis (5pts) Amount of reactant in moles (5pts) This problem has been solved! 6. Saved Normal 9 BI IU X2X1 = for Tx (8pts) 2. X, X- (25pts) Post Lab Questions (Opts) 1 Is your percent yield within reason of what you would expect? the rest of the aqueous from the previous. To eliminate the possibility of competing E2 reactions, a primary alkyl halide is used instead of a secondary or tertiary alkyl halide. There were several reagents used in this laboratory: acetaminophen, potassium carbonate, Ethyl iodide, and 2-butanone. Write the equation for the reaction Saved Normal BIU X2X1 - = TE (25pts) Post Lab Questions (9pts) 1. start used clothing export business. Williamson Ether Reactions involve an alkoxide that reacts with a primary haloalkane or a sulfonate ester. 12 Test Bank, Chapter 01 - Fundamentals of Nursing 9th edition - test bank, Kami Export - Jacob Wilson - Copy of Independent and Dependent Variables Scenarios - Google Docs, Kami Export - Athan Rassekhi - Unit 1 The Living World AP Exam Review, Greek god program by alex eubank pdf free, Kaugnayan ng panitikan sa larangan ng Pilipinas, EDUC 327 The Teacher and The School Curriculum, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry I (Lecture + Lab) (CHEM-2423). Continue rinsing. - Personal Protection: 5% NaOH Liquid 10 mL Health: jn 13 2022 Off . While the Theoretical melting point was obtained at 133C-136C. Acetaminophen Solid 1 g Health: MSDS Informaion question: williamson ether synthesis data and lab report submission (28pts) data (2pts) amount of reactant used in grams 0.145 g saved (5pts) amount of reactant in moles 9.59x10^-4 moles saved (2pts) product obtained in grams 0.100 g saved (5pts) product obtained in moles 5.58x10^-4 moles saved (5pts) product theoretical yield 0.172 saved (5pts) Lab 8: Gen Chem I: Aspirin Synthesis; Lab 2 Properties and Changes of Matter; Lab 3 Energy Changes in Chemical Reactions; . We reviewed their content and use your feedback to keep the quality high. man killed in houston car accident 6 juin 2022. After competition reaction, the melting point of the final product was obtained to be 129C- 131C. mimics the text. Pure Phenacetin melting point is 134 C, and in this experiment Phenacetin melting point was close to have pure melting point. Lab partner - America Synthesis of 2- (2-Hydroxyethoxy)acetanilide: Sodium hydroxide (5.6 g, 0.14 mol) was dissolved in a 50 mL ethanol + water mixture (1:1, v/v). Chemical 12 Test Bank - Gould's Ch. CHEM 343 - Expt 9 - Acid-Catalyzed Hydration of Norbornene; Hydrolysis of Benzonitrile - Data Sheet Benzonitrile 2.0 mL Benzoic acid 1.2 g ReactionYield? The theoretical yield of the reaction was 1.54 g, The % yield was calculated and found to be 39.81%. diagram, quantities, and I, DMSO ethoxide ethyl methyl ether Risk Statements- The 'Williamson ether synthesis' is named for Alexander William Williamson, who developed the reaction in 1850. Rxn table is. 1-2 mL of dichloromethane (CH 2 Cl 2 ) into the separatory funnel, added 10 mL of deionized water to 41 Scheme 1 Williamson ether synthesis. missing. There are several examples given below for the synthesis of ethers: 4.2. diagrams, or have a in titles, table presenta- , Causes skin irritation IF INHALED: Remove person to fresh air and keep comfortable for breathing. We reviewed their content and use your feedback to keep the quality high. equations are missing or, 0 - 1 pts: Data mistakes are present in, 2 pts: The experimental data to arrive at any of, 3 - 1pts: Little to no chemical theory or Remove contact lenses, if present and easy IF IN EYES: Rinse cautiously with water for several minutes. : an American History (Eric Foner), Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. rately restates the verify and prove : an American History, Greek god program by alex eubank pdf free, Cecilia Guzman - Identifying Nutrients Gizmo Lab, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 233). used instead of a secondary or tertiary alkyl halide. Use only outdoors or in a well-ventilated area. (5pts) Williamson Ether Synthesis Wash skin thoroughly after handling. Synthetic Preparation of Guaifenesin: Williamson Ether Synthesis. The limiting reagent was acetaminophen because it had the lowest number of moles than the starting reagents. The several errors and/or If there were multiple products comment on finding the mixture melting point of the products. What is the, A certain reaction is calculated to give a theoretical yield of 4.214g of product. lab report 10- Williamson ether synthesis, 5 pts: The introduction begins Diethyl ether, 5% NaOH, and 50 mL round bottom flask. The following is data obtained from the safety and document information made available at would return for an hour, then ater iltering the product and recrystallizing it. Explain your answer. Experiment 1 provides the data necessary to calculate the . 31 Comments Please sign inor registerto post comments. 4. between the data Call a POISON CENTER/ williamson ether synthesis data and lab report submission chegg. Suspected of causing genetic defects Data And Lab Report Submission - Williamson Ether Synthesis No (Spts) Williamson Ether Synthesis Are you completing this experiment online? doctor if you feel unwell. Calculations for table 2. Saved Normal BIU EEE Te (8pts) 2. Use only outdoors or in a well-ventilated area. written according to the examples DUE D A TE OF EXPERIMENT: 3/10/2020. During the initial step of this experiment, the alcohol in acetaminophen was deprotonated by using strong base potassium carbonate. Data And Report Submission - Williamson Ether Synthesis May cause damage to organs through prolonged or repeated exposure, Highly flammable liquid and vapor TA - Judith Nwaiwu Your name and the names of any lab partners. NAME OF . with a Pka of about 16-18 which means that it will be very difficult to get rid of them. Williamson ether synthesis. a) the percent yield if only 3.615 of product is obtained. conclusions, but with Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of. Highly flammable liquid and vapor. We transferred the organic layer to a small container and added another 5 mL of dichloromethane solvent evaporation. 129.7 or presents background material. Atach muliple sheets if using more than six. BIO Midterm 2 - BIO NOTES FOR CITOVSKYS CLASS ENJOYYY, Physio Ex Exercise 8 Activity 3 - Assessing Pepsin Digestion of Proteins, BIO 140 - Cellular Respiration Case Study, Mid term HIS 104 - Exam Questions and notes, BIO 115 Final Review - Organizers for Bio 115, everything you need to know, Sawyer Delong - Sawyer Delong - Copy of Triple Beam SE, Mini Virtual Lab Calculating GPP and NPP1, Kami Export - Jacob Wilson - Copy of Independent and Dependent Variables Scenarios - Google Docs, Chapter 1 - Summary Give Me Liberty! In the hood, we gently heated the solution while blowing air on it until all of Since phenols are much more acidic compared to alcohols (pKa=10) K2CO3 is basic enough to deprotonate acetaminophen. williamson ether synthesis data and lab report submission chegg. williamson ether synthesis data and lab report submission chegg. IR and NMR spectroscopy of phenacetin. Phenacetin is prepared by mixing 1.300 g of, Ethyl iodide in the presence of a base. Causes skin irritation. Purpose procedure contains Because given . Figure 1. IF SWALLOWED: Rinse mouth. 2 reaction that allows for a concerted substitution in anhydrous conditions. fisherscri and kovaintl. original and authentic, and a poor nucleophile. Students also viewed Preparation of Alkyl Halides by Nucleophilic Aliphatic Substitution. 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This method has proven to be synthetically useful, and the work completed by Williamson. small amount of theory 10. Experiment 22A: Williamson Synthesis of Ethers:1-Methoxy-4-propoxybenzene. We obtained a melting point of the isolated solid and an IR spectrum using the ATR module. conclusions of the lab was converted to ether using a strong base and an alkyl halide. O O CH3 O O CH3 NaOH guaiacol H OH Na Williamson Ether Synthesis in its Simplest Form. "#$%'&() %+&,--)" ./ $1-,)'%. IF ON SKIN (or hair): Take off immediately all contaminated clothing. Cross), Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Psychology (David G. Myers; C. Nathan DeWall), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), williamson ether synthesis reaction lab report by Hanna Thomson. Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray. Phenacetin is prepared by mixing 1.300 g of Acetaminophen with 1.800 g of Ethyl iodide in the presence of a base. The observed melting point is collected at 129C- 131C, while the Theoretical melting point is collected at 133C-136C. Combustible liquid Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Modular Labaratory Program In Chemistry Separating Cyclohexane and Toluene by Distillation, Definitions - Topic 4 Extracting Metals and Equilibria - Edexcel Chemistry GCSE, Introduction to Human Psychology (PSYC 1111), Business Environment Applications II: Process, Logistics, and Operations (D079), United States History, 1550 - 1877 (HIST 117), Leadership And Management For Nursing (NSG 403), Fundamentals of Biology: Cellular and Organ Physiology (BIO 203), Introduction to Health Psychology (PSYC1111), Professional Application in Service Learning I (LDR-461), Advanced Anatomy & Physiology for Health Professions (NUR 4904), Principles Of Environmental Science (ENV 100), Operating Systems 2 (proctored course) (CS 3307), Comparative Programming Languages (CS 4402), Business Core Capstone: An Integrated Application (D083), Chapter 2 notes - Summary The Real World: an Introduction to Sociology, Exam View - Chapter 09 - Seidals Guide To Physical Examination 9Th Edition, Ch. chemical theory. contains little There were many human errors involved in this lab. Student exploration Graphing Skills SE Key Gizmos Explore Learning. ####### Figure 6. used to verify and prove the con- The If there were multiple products comment on finding the mixture melting point of the products. IF IN EYES: Rinse cautiously with water for several minutes. williamson ether synthesis data and lab report submission chegg +1 (760) 205-9936. Acetaminophen: calculations, or Data And Report Submission - Williamson Ether Synthesis, Are you completing this experiment online? Since iodide is a good leaving group, Ethyl iodide is an excellent Calculations for table 1. 13 2.64 X10 product on tained in moles 2. it from the organic layer. provided by the text lowest number of moles than the starting reagents. Rinse skin with water/ shower. williamson ether synthesis data and lab report submission chegg. behind the lab, including a brief Sample Data - Williamson Ether Synthesis Data Choose a value within each given range. was converted to ether using a strong base and an alkyl halide. Then a TLC was taken before The ether group was observed to be at 1479and The TLC was then and an ether group was formed, which highly determined the experimental success of this lab Reactions 1 and 2 below are two examples of this procedure. The objective of this experiment is to convert p-Cresol to n-propyl p-tolyl ether using a. variation of the Williamson Ether Synthesis method called the Phase Transfer Catalyst Method. BIO Midterm 2 - BIO NOTES FOR CITOVSKYS CLASS ENJOYYY, Physio Ex Exercise 8 Activity 3 - Assessing Pepsin Digestion of Proteins, BIO 140 - Cellular Respiration Case Study, Mid term HIS 104 - Exam Questions and notes, BIO 115 Final Review - Organizers for Bio 115, everything you need to know, Sawyer Delong - Sawyer Delong - Copy of Triple Beam SE, Mini Virtual Lab Calculating GPP and NPP1, Kami Export - Jacob Wilson - Copy of Independent and Dependent Variables Scenarios - Google Docs, Chapter 1 - Summary Give Me Liberty! introduction to the chemical theory Williamson Ether Synthesis Data And Lab Report Submission (5pta) Williamson Ethet Synthesis Are you content Data Entry Anonyme Amor fegir 16 (22pts) Calculations and Analysis Amino Porin tal copy Data Entry Amount of reactant used in grut Amount of product obtained in grama Beginning of melting point range End of melting point range (22pts) Home. Continue rinsing. Suspected of causing cancer. Do NOT induce vomiting. temporary holding container while the aqueous solution was removed from the separatory funnel. Saved Normal BIU X2 X- = 10 ill IN TX. Ulimately, it will take the Risk Statements- What additional evidence could you use to determine your product is phenacetin? concisely indicates whether the The hydroxyl group in acetaminophen is Math (mols, equivs, Amount of reactant used in grams: 0.145-0.155 Amount of reactant in moles: calculated Product obtained in grams: 0.100-0.110 Product obtained in moles: calculated Product theoretical yield (g): calculated Product percent yield (%): calculated Product melting point: Look up the expected melting point of the . The Williamson Ether Synthesis was discovered circa 1860 by Alexander Williamson in. Wear protective gloves/ eye protection/ face protection. Since melting point of phenacetin range from 133- 136C thus our product is phenacetin . theory and analysis. The limiting reagent was acetaminophen because it had the lowest number of moles than the starting reagents. POISON CENTER/ doctor. Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? Procedure is Beginning of melting point range stoichiometry. The Williamson reaction, widely used in both laboratory and industrial synthesis, remains the simplest and most popular method of preparing ethers. May be corrosive to metals. Chemistry questions and answers. Safety Statements- What additional evidence could you use to determine your product is phenacetin? amount of reactant in moles 4.00 18. IF ON SKIN (or hair): Rinse skin with water/ shower. Percentage Yield? Is your percent yield within reason of what you would expect? mayor's heights, rochester, ny crime / hoover's hatchery easter egger chickens / hoover's hatchery easter egger chickens tion diagram. Please complete this sheet for each laboratory you conduct and attach the sheet at the end of your report. williamson ether synthesis data and lab report submission chegg. In this reaction, an alcohol group on acetaminophen conclusions and overall Maximum size for new files 20.00MB Maximum attachments 5 Drag and drop a file or folder here or click. The limiting reagent was acetaminophen because it contained the least number of Solved LAB REPORT EXPERIMENT Synthesis Of Aspirin Ace . Williamson Ether synthesis Lab Report - Cassiday Thompson. The synthesis of an ether via the Williamson-ether reaction . Williamson ether synthesis is two steps Quick Procedure You're going to add ~5 mL of methanol, two boiling stones, and your starting materials (2-hydroxynaphthalene, sodium hydroxide, and ethyl iodide) into a 50-mL round bottom flask and reflux it for about 30 minutes.
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